Any help please. On the Chemistry of Tris- (acetylacetate) Chromium (III)

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Dakingnick
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Any help please. On the Chemistry of Tris- (acetylacetate) Chromium (III)

Post by Dakingnick »

How to determine the concentration of CrO²–4 from the calibration curve.
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ChenBeier
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Re: Any help please. On the Chemistry of Tris- (acetylacetate) Chromium (III)

Post by ChenBeier »

To less information.
Which Kind of analysis method?
Dakingnick
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Re: Any help please. On the Chemistry of Tris- (acetylacetate) Chromium (III)

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Quantitative analysis. Where you determine the concentration of CrO²- 4 anion . Using the method of quantitative conversion of Cr(aCaC)3 to a yellow CrO²- 4 anion. Using the maximum absorbance 365nm. FTIR.
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Re: Any help please. On the Chemistry of Tris- (acetylacetate) Chromium (III)

Post by Dakingnick »

That's the experiment, hope so it's clear
That's the experiment, hope so it's clear
IMG_20231211_235650_091.jpg (73.03 KiB) Viewed 3892 times
IMG_20231211_235702_455.jpg
IMG_20231211_235702_455.jpg (68.52 KiB) Viewed 3892 times
That's the experiment, hope so it's clear
That's the experiment, hope so it's clear
IMG_20231211_235650_091.jpg (73.03 KiB) Viewed 3892 times
Dakingnick
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Re: Any help please. On the Chemistry of Tris- (acetylacetate) Chromium (III)

Post by Dakingnick »

The Chromium analysis part
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ChenBeier
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Re: Any help please. On the Chemistry of Tris- (acetylacetate) Chromium (III)

Post by ChenBeier »

The method is written, but to prepare the calibration curve is not in your paper. You have to prepare some samples with different content of CrO4 2- and measure the absorbance to get the calibration curve.
Later you use the unknown sample to get its content by measuring the absorbance.
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