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Is this reaction possible in room temperature?
Posted: Mon Sep 11, 2023 2:32 am
by Jothi Manikandan
AlCl3 + NH4Cl + 4 NaOH = AlN + 4 NaCl + 4 H2O
kindly help me in this.
Re: Is this reaction possible in room temperature?
Posted: Mon Sep 11, 2023 2:50 am
by ChenBeier
No, AlN goes under hydrolysis if wet.
Synthesis need temperature up to 1600 °C
https://en.m.wikipedia.org/wiki/Aluminium_nitride
Re: Is this reaction possible in room temperature?
Posted: Mon Sep 11, 2023 3:08 am
by Jothi Manikandan
Thankyou very much for the reply. How to do doping of Iron in commercial AlN powder?
Re: Is this reaction possible in room temperature?
Posted: Mon Sep 11, 2023 3:13 am
by ChenBeier
Re: Is this reaction possible in room temperature?
Posted: Mon Sep 11, 2023 3:19 am
by Jothi Manikandan
Thankyou very much for your help. I will go through this. Still, I am checking some wet chemical procedures like Hydrothermal, since I don't have the facility to reach very high temperatures. If there are any suggestions for low temperature techniques, please enlighten.
