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Re: Help Me!! I havew to refine palladium !

Posted: Mon Jun 14, 2021 11:06 am
by aliossi001122
i saw one video that i have to put it in oven to heat till it becomes black and than melt can you confirm if that fine

Re: Help Me!! I havew to refine palladium !

Posted: Mon Jun 14, 2021 11:12 am
by ChenBeier
But I think this will get only PdO. Above 750 °C it will decompose to Pd. Under nitrogen or Argon atmosphäre you can get it after cooling down.

Re: Help Me!! I havew to refine palladium !

Posted: Mon Jun 14, 2021 11:23 am
by aliossi001122
what dou you think is the best way to take pd from that filtering paper

Re: Help Me!! I havew to refine palladium !

Posted: Mon Jun 14, 2021 11:42 am
by ChenBeier
I think in the oven the paper will burn anyway.

Re: Help Me!! I havew to refine palladium !

Posted: Thu Jun 17, 2021 6:09 am
by aliossi001122
Thanks to you we now know all the procedures . except turning dimethylglyoxime palladium complex into metallic palladium .
We try melting with induction but we failed we try with oxygen torch still a fail .
what do you think that we have to do to get into metal .
Thanks for all responses .

Re: Help Me!! I havew to refine palladium !

Posted: Thu Jun 17, 2021 8:17 am
by ChenBeier
You need Reduction what I told before.

Re: Help Me!! I havew to refine palladium !

Posted: Thu Jun 17, 2021 11:00 am
by aliossi001122
Ok i got that , we have to avoid oxidations in argon or hydrogen atmosphere. But what do you think that is the right temperature .
Will under melting point work .?

Re: Help Me!! I havew to refine palladium !

Posted: Thu Jun 17, 2021 11:15 am
by ChenBeier
I dont know, I would acid to use the complex. If Meeting a lot of organic Material wie decompose an dprobably you get again PdC. Better is to have the solution of Pd 2+ and add reducer compound. Maybe Magnesium or zinc.

Re: Help Me!! I havew to refine palladium !

Posted: Fri Jun 18, 2021 3:01 pm
by mitali
how do i post my question? i am new here.

Re: Help Me!! I havew to refine palladium !

Posted: Fri Jun 18, 2021 9:28 pm
by ChenBeier
viewforum.php?f=10

Klick new topic above left.

Re: Help Me!! I havew to refine palladium !

Posted: Tue Nov 02, 2021 6:40 pm
by jebbasha
Burning at high temperature get PdO and CO2