Help Me!! I havew to refine palladium !

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aliossi001122
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Re: Help Me!! I havew to refine palladium !

Post by aliossi001122 »

i saw one video that i have to put it in oven to heat till it becomes black and than melt can you confirm if that fine
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ChenBeier
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Re: Help Me!! I havew to refine palladium !

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But I think this will get only PdO. Above 750 °C it will decompose to Pd. Under nitrogen or Argon atmosphäre you can get it after cooling down.
aliossi001122
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Re: Help Me!! I havew to refine palladium !

Post by aliossi001122 »

what dou you think is the best way to take pd from that filtering paper
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ChenBeier
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Re: Help Me!! I havew to refine palladium !

Post by ChenBeier »

I think in the oven the paper will burn anyway.
aliossi001122
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Re: Help Me!! I havew to refine palladium !

Post by aliossi001122 »

Thanks to you we now know all the procedures . except turning dimethylglyoxime palladium complex into metallic palladium .
We try melting with induction but we failed we try with oxygen torch still a fail .
what do you think that we have to do to get into metal .
Thanks for all responses .
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ChenBeier
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Re: Help Me!! I havew to refine palladium !

Post by ChenBeier »

You need Reduction what I told before.
aliossi001122
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Re: Help Me!! I havew to refine palladium !

Post by aliossi001122 »

Ok i got that , we have to avoid oxidations in argon or hydrogen atmosphere. But what do you think that is the right temperature .
Will under melting point work .?
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ChenBeier
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Re: Help Me!! I havew to refine palladium !

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I dont know, I would acid to use the complex. If Meeting a lot of organic Material wie decompose an dprobably you get again PdC. Better is to have the solution of Pd 2+ and add reducer compound. Maybe Magnesium or zinc.
mitali
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Re: Help Me!! I havew to refine palladium !

Post by mitali »

how do i post my question? i am new here.
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ChenBeier
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Re: Help Me!! I havew to refine palladium !

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viewforum.php?f=10

Klick new topic above left.
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