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by Kelrash
Wed Mar 08, 2017 9:44 am
Forum: Chemistry forum
Topic: Purification of volatile aldehydes
Replies: 0
Views: 5241

Purification of volatile aldehydes

Hey, I am trying to get 4-pentenal from 4-penten-1-ol. Swern or DMP work but the work up/purification is the problem. I want to use the newly formed aldehyde in a reaction involving LDA in the next step at -78°C so I need it to be in THF and not DCM. Distillation usually lead to either the product ...